Giancotti Rag. Giuseppe Commercio Ingrosso di Olii, Vini e Prodotti Tipici (@3720-12 Viale dei Normanni, 48 88069 Squillace (CZ Sample Number: 4.657/14 Tests Beginning Date: 05/09/2014 Receipt date: 05/09/2014 Tests Term Date: 10/09/2014 Check Temperature C: 23.3 Temperature in Accordance: Yes Goods Category: Declared Product: Sample Description: Sample Label: Seal Description: Sample Amount: Paking: Sampling Procedure: 0000 - ALIMENTARY OILS 01. Extra Virgin Olive Oil Extra Virgin Olive Oil N 19 None Rizziconi 10/09/2014 Sampling Date: 05/09/2014 Report Sampling Number: / 250 ml Sample Return: No 1 bottle in glass with cap to screw (* By the customer The analytical results refer to the sample tested. This document may only be reproduced in whole. Partial reproduction must be authorized with written approval of our Laboratory. A Counter is stored in temperature conditions likely to maintain its integrity for a period between 5 and 15 days in relation to the required tests and its perishability. All the data are stored for analysis over a period of four years. The accreditation of the laboratory does not constitute endorsement of the product by the Accreditation Body. Any assessment given are not part of the test accredited by Accredia. The test results can not be used for advertising purposes (* - Tests not accredited Accredia. FL = Annotation that indicates a value beyond the regulatory limit. U.M. = Units. ----------------------------------- CHEMICAL TESTS ---------------------------------- The expanded uncertainty is calculated with a probability level of 95%, coverage factor k> = 2 and degrees of freedom> 9. The results reported in this test report is produced to n. 1 race. Legend: LRi = Lowest Detection Limit for the method. - NV= Not Valuable because < LRi. ------------------------------- MICROBIOLOGICAL TESTS ------------------------ The uncertainty of measurement is expressed as expanded uncertainty with a confidence level of 95% and the coverage factor k = 2. The results reported in this test report is produced to n. 1 race. Legend: " " = micro-organisms are present but are below the indicated value. " # " = micro-organisms are lower than the value indicated. - " @ " = Estimated counts. 0046-A0 - Free fatty acids, cold method, % m/m 0.31 ± 0.05 Max 0.8 (29 Cod. Met. / Metod: 0046-00 / ECC Reg No 2568/1991 of 11 July 1991 OJ L248 05/09/1991 Ann II EC Reg No 702/2007 of 21 June 2007 OJ L161 22/06/2007 0050-A0 - Peroxide value, meq.o2/kg. oil 3.60 ± 0.7 Max 20 (29 Cod. Met. / Metod: 0050-00 - ECC Reg No 2568/1991 of 11 July 1991 OJ L248 05/09/1991 Ann III 0052-A0 - Spectrophotometric investigation in the ultraviolet Cod. Met. / Metod: 0052-00 / EEC Reg No 2568/1991 of 11 July 1991 OJ L248 05/09/1991 Ann IX EEC Reg No 183/1993 of 29 January 1993 OJ L22 30/01/1993 Page 1 of 17
Giancotti Rag. Giuseppe Commercio Ingrosso di Olii, Vini e Prodotti Tipici (@3720-12 - K232 1.75 ± 0.10 Max 2.5 (29 - K266 0.11 ± 0.02 - K270 0.11 ± 0.02 Max 0.22 (29 - K274 0.10 ± 0.02 - Delta K -0.00 ± 0.003 Max 0.01 (29 0047-A0 - Individual and total sterols content, % Cod. Met. / Metod: 0047-00 / ECC Reg No 2568/1991 of 11 July 1991 OJ L248 05/09/1991 Ann V EEC Reg No 183/1993 of 29 January 1993 OJ L22 30/01/1993 - Cholesterol 0.10 ± 0.07 Max 0.5 (29 - Brassicasterol 0.00 Max 0.1 (29-24-Methylencholesterol 0.13 - Campesterol 1.95 ± 0.10 Max 4 (29 - Campestanol 0.15 - Stigmasterol 0.80 ± 0.08 - Delta-7 Campesterol 0.00 - Delta-5,23 Stigmastadienol 0.00 - Clerosterol 1.07 - Betasitosterol 81.47 - Sitostanol 0.69 - Delta-5 Avenasterol 12.04 - Delta-5,24 Stigmastadienol 0.86 - Delta-7 Stigmastenol 0.18 ± 0.05 Max 0.5 (29 - Delta-7 Avenasterol 0.56 - TOTAL BETASITOSTEROL, % 96.14 ± 0.30 - TOTAL STEROLS CONTENT, mg/kg 1214 ± 65.0 Min 1000 (29 0048-A0 - Erythrodiol and uvaol, % Total Sterols 1.85 Cod. Met. / Metod: 0047-02 - EEC Reg No 2568/1991 of 11 July 1991 OJ L248 05/09/1991 Ann VI 0177-A0 - Waxes (C42+C44+C46 - mg/kg 35.40 ± 5.0 Max 150 (29 Cod. Met. / Metod: 0177-00 - EEC Reg No 2568/1991 of 11 July 1991 OJ L248 05/09/1991 Ann IV EC Reg No 702/2007 of 21 June 2007 OJ L161 22/06/2007 0177-A1 - Waxes (C40+C42+C44+C46 - mg/kg 63.50 ± 5.0 Cod. Met. / Metod: 0177-00 - EEC Reg No 2568/1991 of 11 July 1991 OJ L248 05/09/1991 Ann IV EC Reg No 702/2007 of 21 June 2007 OJ L161 22/06/2007 0049-A0 - Methyl esters of fatty acids, in % Cod. Met. / Metod: 0049-00 / ECC Reg No 2568/1991 of 11 July 1991 OJ L248 05/09/1991 Ann XA ECC Reg No 1492/1992 of 25 May 1992 OJ L150 02/06/1992 EC Reg No 702/2007 of 21 June 2007 OJ L161 22/06/2007 - C12:0 - Lauric acid < 0,01 - C14:0 - Myristic acid 0.01 ± 0.01 Max 0.03 (29 - C16:0 - Palmitic acid 14.24 ± 0.42 [7.5; 20] (29 - C16:1 - Palmitoleic acid 1.53 ± 0.05 [0.3; 3.5] (29 - C17:0 - Heptadecanoic acid 0.19 ± 0.03 - C17:1 - Heptadecenoic acid 0.30 ± 0.04 Max 0.3 (29 - C18:0 - Stearic acid 2.51 ± 0.15 [0.5; 5] (29 - C18:1 - Oleic acid 73.90 ± 0.60 [55; 83] (29 Page 2 of 17
Giancotti Rag. Giuseppe Commercio Ingrosso di Olii, Vini e Prodotti Tipici (@3720-12 - C18:2 - Linoleic acid 5.92 ± 0.10 [3.5; 21] (29 - C20:0 - Arachidic acid 0.44 ± 0.05 Max 0.6 (29 - C18:3 - Linolenic acid 0.49 ± 0.07 Max 1 (29 - C20:1 - Eicosenoic acid 0.28 ± 0.05 Max 0.4 (29 - C22:0 - Behenic acid 0.12 ± 0.03 Max 0.2 (29 - C22:1 - Erucic acid < 0,01 - C24:0 - Lignoceric acid 0.06 ± 0.01 Max 0.2 (29 0049-A1 - Trans fatty acid content, % Cod. Met. / Metod: 0049-00 / ECC Reg No 2568/1991 of 11 July 1991 OJ L248 05/09/1991 Ann XA ECC Reg No 1492/1992 of 25 May 1992 OJ L150 02/06/1992 EC Reg No 702/2007 of 21 June 2007 OJ L161 22/06/2007 - C18:1 - (Elaidinic < 0,01 Max 0.05 (29 - C18:2 + C18:3 < 0,01 Max 0.05 (29 0053-A0 - Stigmastadienes, ppm Cod. Met. / Metod: 0053-00 - ECC Reg No 2568/1991 of 11 July 1991 OJ L248 05/09/1991 Ann XVII EC Reg No 656/1995 of 28 March 1995 OJ L69 29/03/1995 - Stigmasta 3,5 dien 0.01 Max 0.05 (29 0054-A0 - Triglycerides with ECN42, % Cod. Met. / Metod: 0054-00 - ECC Reg No 2568/1991 of 11 July 1991 OJ L248 05/09/1991 Ann XVIII EC Reg No 2472/1997 of 11 December 1997 OJ L28 12/12/1997 EC Reg No 282/1998 of 3 March 1998 OJ L28 04/02/1998 - LLL 0.04 - Sum ECN-42 HPLC 0.22 - Theoretical ECN-42 0.24 - Difference ECN42 < 0,00 Max 0.2 (29 0175-A0 - Determ. of Methyl and Ethyl Esters of Fatty Acids (FAME e FAEE Cod. Met. / Metod: 0175-00 / Reg (UE No 61/2011 24/01/2011 GU CEE L23/1 27/01/2011 - Methyl Palmitate - in mg/kg 1.0 - Ethyl Palmitate - in mg/kg 0.9 - Methyl Linoleate - in mg/kg 0.2 - Methyl Oleate - in mg/kg 3.2 - Methyl Stearate - in mg/kg 0.3 - Ethyl Linoleate - in mg/kg 0.4 - Ethyl Oleate - in mg/kg 4.0 - Ethyl Stearate - in mg/kg 0.3 - Total Methyl Esters - FAME - in mg/kg 4.2 - Total Ethyl Esters - FAEE - in mg/kg 4.9 Max 40 (29 - Total FAME + FAEE - in mg/kg 9.0 - FAEE / FAME 1.2 - FAME / FAEE 0.9 0354-00(* - Lead in mg/kg < 0,01 Cod. Met. / Metod: EPA 3051A + ISO 8294-1994 0356-00(* - Arsenic in mg/kg < 0,01 Cod. Met. / Metod: EPA 3051A + ISO 8294-1994 Page 3 of 17
Giancotti Rag. Giuseppe Commercio Ingrosso di Olii, Vini e Prodotti Tipici (@3720-12 0051-A1(* - Halogenated Solvents - in ppm o mg/kg - LRI = 0.001 Cod. Met. / Metod: 0051-00 / Reg. C.E.E. n. 2568/91 e succ. modif., All.XI - LRi 0,01 mg/kg - Trichlorofluoromethane < 0,01 Max 0.1 (15 - Chloroform < 0,01 Max 0.1 (15-1,1,1-Trichloroethane < 0,01 Max 0.1 (15 - Tetraclhorometane < 0,01 Max 0.1 (15 - Trichloroethylene < 0,01 Max 0.1 (15 - Bromodichloromethane < 0,01 Max 0.1 (15 - Tethrachloroethylene < 0,01 Max 0.1 (15 - Dibromochloromethane < 0,01 Max 0.1 (15 - Bromophorm < 0,01 - Other solvents < 0,01 - Total solvents < 0,01 Max 0.2 (15 0300-00(* - AFLATOXINS - in µg/kg o ppb - LRI = 0,1ppb Cod. Met. / Metod: 0000-00 / Metodo HPLC - con Rivelatore Spettrofluorimetrico - (* G2 < 0.1 - (* B1 < 0.1 - (* G1 < 0.1 - (* B2 < 0.1 - (* Sum G2 - B1 - G1 - B2 < 0.1 0179-00(* - Unsaponifiable matter (In petroleum Ether - in % 1.3 Cod. Met. / Metod: 0000-00 / Metodo Norme Grassi e Derivati C12-1976. 0166-A0(* - Water content and volatile substances ( a 105 C. - in % 0.10 ± 0.02 Cod. Met. / Metod: 0166-00 / Metodo N.G.D. C3-1976. 0167-A0(* - Insoluble impurities in Ether petroleum - in % < 0.05 Cod. Met. / Metod: 0167-00 / Metodo: Norme Grassi e Derivati C7-1976. 0360-00 (* - TOTAL SOLVENTS - How to n-hexane, in mg / kg < 0,10 Cod. Met. / Metod: 0360-00 / ISO 9832-1992 0200-02A(* - (PAHs Polycyclic Aromatic Hidrocarbons (light - in ppb o µg/kg- LRI = 0.1ppb Cod. Met. / Metod: 0200-00 / ISO 13887-1998 - (* - Phenanthrene 2.4 - (* - Anthracene 0.3 - (* - Fluorene 0.7 - (* - Pyrene 0.4 - (* - ( - Benzo (a anthracene < 0,1 - (* - ( - Chrysene 0.2 - (* - Sum PHAs (Light 4.0 0046-05(* - Acidity as mg/g KOH 0.000 Cod. Met. / Metod: 0046-05 / Internal Method Page 4 of 17
Giancotti Rag. Giuseppe Commercio Ingrosso di Olii, Vini e Prodotti Tipici (@3720-12 0000-00(* - in mg/kg o ppm - LOQ = 0,01 Cod. Met. / Metod: 0001-00 / UNI EN 1528-1:1997 + UNI EN 1528-2:1997 + UNI EN 1528-3:1997 + UNI EN 1528-4:1997-2,4 D < 0,01-2,4 DDD - (o Mitotane o-p < 0,01-4,4 DDD - p-p < 0,01-2,4 DDE - p-p < 0,01-4,4 DDE p-p < 0,01-2,4 DDT - o-p < 0,01-4,4 DDT - p-p < 0,01-2,4-Dichlorophenoxyacetic acid < 0,01-3,5-Dichloroaniline < 0,01-3-Idrossucarbofuran < 0,01-2-Phenylphenol < 0,01 - Abamectin < 0,01 - Acephate < 0,01 - Acetamiprid < 0,01 - Acetochlor < 0,01 - Acibenzolar S Methyl < 0,01 - Aclonifen < 0,01 - Acrinathrin < 0,01 - Alachlor < 0,01 - Albendazole < 0,01 - Aldicarb < 0,01 - Aldicarb sulfone < 0,01 - Aldicarb sulfoxide < 0,01 - Aldicarb (sum of aldicarb, its sulfoxide and its sulfone, expressed as < 0,01 Max 0.1 (175 aldicarb - Aldoxicarb < 0,01 - Aldrin < 0,01 - Alletrina < 0,01 - Ametryn < 0,01 - Aminocarb < 0,01 - Amitraz < 0,01 - Anilazine < 0,01 - Asulam < 0,01 - Atraton < 0,01 - Atrazine o Desethylatrazine < 0,01 - Azaconazole < 0,01 - Azinphos Ethyl < 0,01 Max 0.1 (161 - Azinphos Methyl < 0,01 - (* Azobenzene < 0,01 - Azocyclotin < 0,01 - Azoxystrobin < 0,01 - Barban < 0,01 - Benalaxyl < 0,01 - Bendiocarb < 0,01 - Benfuracarb < 0,01 - Benfluralin < 0,01 Page 5 of 17
Giancotti Rag. Giuseppe Commercio Ingrosso di Olii, Vini e Prodotti Tipici (@3720-12 - Benomyl < 0,01 - Benoxacor < 0,01 - Bentazone < 0,01 - Benthiavalicarb-isopropyl < 0,01 - Benzoximate < 0,01 - Beta BHC < 0,01 - Bifenox < 0,01 - Bifenthrin < 0,01 - Biphenyl < 0,01 - bitertanol < 0,01 - Boscalid < 0,01 - Bromacil < 0,01 - Bromophos Ethyl < 0,01 - Bromophos Methyl < 0,01 - Bromopropylate < 0,01 - Bromoxynil Octanoato < 0,01 - Bromuconazole < 0,01 - Bupirimate (o Pirimidinol < 0,01 - Buprofezin < 0,01 - Butaclor < 0,01 - Butafenacil < 0,01 - Butocarboxim < 0,01 - Cadusafos < 0,01 - Captafol < 0,01 - Captan < 0,01 - Carbaryl < 0,01 - Carbendazim < 0,01 - Carbofuran < 0,01 - Carbophenothion < 0,01 - Carbosulfan < 0,01 - Carboxina < 0,01 - Carfentrazone-Ethyl < 0,01 - Chinomethionate < 0,01 - Chlomazone < 0,01 - Chlorantraniliprole < 0,01 - Chlorbromuron < 0,01 - Chlorbufam < 0,01 - Chlorfenapyr < 0,01 - Chlordane (cis + trans < 0,01 - Chlorfenson < 0,01 - Chlorfentezine < 0,01 - Chlorfenvinphos < 0,01 - Chlorfiurenol < 0,01 - Chlormephos < 0,01 - Chlorobenzilate < 0,01 - Chloropropylate < 0,01 - Chloroneb < 0,01 - Chlorothalonil < 0,01 Page 6 of 17
Giancotti Rag. Giuseppe Commercio Ingrosso di Olii, Vini e Prodotti Tipici (@3720-12 - Chlorofenapyr < 0,01 - Chlorofluazuron < 0,01 - Chloridazon < 0,01 - Chlorpropham < 0,01 - Chlorpyrifos Ethyl < 0,01 - Chlorpyrifos Methyl < 0,01 - Chlorsulfuron < 0,01 - Chlortiamide < 0,01 - Chlorthal Dimethyl < 0,01 - Chlortion < 0,01 - Chlorthalonil < 0,01 - Chlorthiophos < 0,01 - Chlortoluron o Chlorotoluron < 0,01 Max 0.25 (161 - Chlozolinanate < 0,01 - Clethodim < 0,01 - Clodinafop-Propargyl < 0,01 - Clomazone < 0,01 - Clopyralid < 0,01 - Clothianidin < 0,01 - Coumaphos < 0,01 - Crimidine < 0,01 - Cyanophos < 0,01 - Cyazofamid < 0,01 - Cycloate < 0,01 - Cycloxydim < 0,01 - Cyhalofop-Butyl < 0,01 - Cyanazina < 0,01 - Cyfluthrins < 0,01 - Cyhalotrin (Lambda < 0,01 - Cyhexatin < 0,01 - Cymiazolo < 0,01 - Cymoxanil < 0,01 - Cypermethrins < 0,01 - Cyproconazole < 0,01 - Cyprodinil < 0,01 - Cyromazine < 0.01 Max 0.25 (174 - Daminozid < 0,01 - Deet < 0,01 - Delta BHC < 0,01 - Deltamethrin < 0,01 Max 5 (160 - Demeteo-S-Methyl < 0,01 - Desmethryn < 0,01 - Demeton-S-Methylsulfone < 0,01 - Desetil-Terbutilazina < 0,01 - Desmedipham < 0,01 - Diafenthiuron < 0,01 - Dialifor o Dialifos < 0,01 - Diazinon < 0,01 Page 7 of 17
Giancotti Rag. Giuseppe Commercio Ingrosso di Olii, Vini e Prodotti Tipici (@3720-12 - Dicamba < 0,01 - Dichlobenil < 0,01 - Dichlofenthion < 0,01 - Dichlofluanid < 0,01 - Dichlorophenylisocyanate 3-4 < 0,01 - Diclofop Methyl < 0,01 - Dichlorvos < 0,01 - Diclobutrazol < 0,01 - Dicloran < 0,01 - Dicofol < 0,01 - Dicrotophos < 0,01 - Dieldrin < 0,01 - Diethofencarb < 0,01 - Difenoconazole < 0,01 - Diflubenzuron < 0,01 - Diflufenican < 0,01 - Dimepiperate < 0,01 - Dimethenamid < 0,01 - Dimethoate < 0,01 - Dimetomorph (cis + trans < 0,01 - Dimoxystrobin < 0,01 - Diniconazole < 0,01 - Dinitramine < 0,01 - Dinocap < 0,01 - Dinotefuran < 0,01 - Dioxacarb < 0,01 - Dioxathion < 0,01 - Diphenamid < 0,01 - Diphenylamina < 0,01 - Dipropetryn < 0,01 - Diquat < 0,01 - Disulfoton < 0,01 - Disulfoton Sulfone < 0,01 - Disulfoton Sulfoxide < 0,01 - Disulfoton (sum of disulfoton, disulfoton sulfoxide and disulfoton < 0,01 Max 0.1 (176 sulfone - Ditalimphos < 0,01 - Dithianon < 0,01 - Diuron < 0,01 Max 0.1 (198 - Dodine < 0,01 - Emamectin < 0,01 - Endosulfan < 0,01 - Endosulfan (cis + trans < 0,01 - Endosulfan Solfato < 0,01 - Endrin < 0,01 - Endrin aldeide < 0,01 - Epoxiconazol < 0,01 - EPTC < 0,01 Page 8 of 17
Giancotti Rag. Giuseppe Commercio Ingrosso di Olii, Vini e Prodotti Tipici (@3720-12 - Esaclorobenzene HCB < 0,01 - Esfenvalerate < 0,01 - Etaconazole < 0,01 - Ethalfluralin < 0,01 - Etephon < 0,01 - Ethiofencarb < 0,01 - Ethiofencarb-Sulfone < 0,01 - Ethiofencarb-Sulfoxide < 0,01 - Ethofumesate < 0,01 - Ethoprophos < 0,01 - Ethoxyquin < 0,01 - Ethylan < 0,01 - Ethyl p-nitrophenyl phenylphosphorothioate (EPN < 0,01 - Etofenprox < 0,01 Max 0.05 (173 - Etoxazol < 0,01 - Etridiazol < 0,01 - Etrimfos < 0,01 - Famoxadone < 0,01 - Famphur < 0,01 - Fenamidone < 0,01 - Fenamiphos < 0,01 - Fenarimol < 0,01 - Fenazaquin < 0,01 - Fenbuconazole < 0,01 - Fenbutatin oxide < 0,01 - Fenflutrhin < 0,01 - Fenhexamid < 0,01 - Fenitrothion < 0,01 - Fenobucarb < 0,01 - Fenothiocarb < 0,01 - Fenoxaprop P Ethyl < 0,01 - Fenoxycarb < 0,01 - Fenpropathrin < 0,01 - Fenpropidin < 0,01 - Fenpropimorph < 0,01 - Fenpyroximate < 0,01 - Fenson < 0,01 - Fensulfothion < 0,01 - Fenthion < 0,01 - Fenthion-Oxon-Sulfoxide < 0,01 - Fenthion-Sulfone < 0,01 - Fenthion-Sulfoxide < 0,01 - Fenthion (fenthion and its oxigen analogue, their sulfoxides and < 0,01 Max 0.05 (175 sulfone expr. as parent - Fentin < 0,01 - Fentin-acetate < 0,01 - Fentin Hydroxide < 0,01 - Fenvalerate < 0,01 Page 9 of 17
Giancotti Rag. Giuseppe Commercio Ingrosso di Olii, Vini e Prodotti Tipici (@3720-12 - Ferclorfenuron < 0,01 - Fipronil < 0,01 - Flonicamid < 0,01 - Fluazifop Butyl < 0,01 - Fluazifop P Butyl < 0,01 - Fluazinam < 0,01 - Fluchloralin < 0,01 - Flucicloxuron < 0,01 - Flucythrinate < 0,01 - Fludioxonil < 0,01 - Flufenacet < 0,01 - Flufenoxuron < 0,01 - Flumioxazin < 0,01 - Fluopicolid < 0,01 - Fluotrimazole < 0,01 - Fluoxastrobin < 0,01 - Fluquinconazole < 0,01 - Flurochloridone < 0,01 - Flusilazole < 0,01 - Fluthiacet-Methyl < 0,01 - Flutolanil < 0,01 - Flutriafol < 0,01 - Fluvalinate Tau < 0,01 - Folpet < 0,01 Max 0.1 (184 - Fonofos < 0,01 - Forchlorfenuron < 0,01 - Formetanat < 0,01 - Formothion < 0,01 - Fosthiazat < 0,01 - Fuberidazole < 0,01 - Furalaxyl < 0,01 - Furathiocarb < 0,01 - Halfenprox < 0,01 - Haloxyfop Ethoxy Ethyl < 0,01 - Haloxyfop Methyl < 0,01 - Haloxyfop -R-Methyl < 0,01 - Heptachlor < 0,01 - Heptachlor Epoxide < 0,01 - Heptachlor (sum of heptachlor and heptachlor epoxide expressed as < 0,01 Max 0.05 (161 heptachlor - Heptenophos < 0,01 - Hexaconazole < 0,01 - Hexaflumuron < 0,01 - Hexythiazox < 0,01 - Imazalil < 0,01 - Imazametabenz-Methyl < 0,01 - Imazamox < 0,01 - Imazethapyr < 0,01 Page 10 of 17
Giancotti Rag. Giuseppe Commercio Ingrosso di Olii, Vini e Prodotti Tipici (@3720-12 - Imidacloprid < 0,01 - Indoxacarb < 0,01 - Iodofenfos < 0,01 - Ioxynil < 0,01 - Iprobenfos < 0,01 - Iprodione < 0,01 Max 0.1 (161 - Iprovalicarb < 0,01 - Isazophos < 0,01 - Isocarbophos < 0,01 - Isodrin < 0,01 - Isofenphos < 0,01 - Isofenphos-methyl < 0,01 - Isoprocarb < 0,01 - Isopropalin < 0,01 - Isoproturon < 0,01 Max 0.25 (161 - Isoxaben < 0,01 - Isoxaflutole < 0,01 - Isoxathion < 0,01 - Kresoxim Methyl < 0,01 - Lenacil < 0,01 - Leptophos < 0,01 - Lindan < 0,01 - Linuron < 0,01 - Lufenuron < 0,01 - Malaoxon < 0,01 - Malathion < 0,01 - Mandipropamid < 0,01 - MCPA < 0,01 - Mecarbam < 0,01 - Mecoprop-P < 0,01 - Mefenpyr-Diethyl < 0,01 - Mepanipyrim < 0,01 - Mepronil < 0,01 - Metalaxyl < 0,01 - Metamitron < 0,01 - Metazachlor < 0,01 - Metconazole < 0,01 - Methabenzthiazuron < 0,01 - Methacrifos < 0,01 - Methamidophos < 0,01 - Methidathion < 0,01 - Methiocarb < 0,01 - Methiocarb Sulfone < 0,01 - Methiocarb Sulfoxide < 0,01 - Methiocarb (sum of methiocarb and methiocarb sulfoxide and sulfone, < 0,01 Max 1 (155 expressed as methiocarb - Methomyl < 0,01 - Methoprothryne < 0,01 Page 11 of 17
Giancotti Rag. Giuseppe Commercio Ingrosso di Olii, Vini e Prodotti Tipici (@3720-12 - methoxychlor < 0,01 - Methoxyfenozide < 0,01 - Metobromuron < 0,01 - Metoxuron < 0,01 - Metolachlor < 0,01 - Metosulam < 0,01 - Metrafenon < 0,01 - Metribuzin < 0,01 - Metsulfuron-Methyl < 0,01 - Mevinphos < 0,01 - Mirex < 0,01 - Monocrotophos < 0,01 - Molinate < 0,01 - Myclobutanil < 0,01 Max 0.1 (161 - Naled < 0,01 - Naptalam < 0,01 - Neburon < 0,01 - Nicosulfuron < 0,01 - Napropamide < 0,01 - Nitepyram < 0,01 - Nitralin < 0,01 - Nitrofen < 0,01 - Nitrothal Isopropyl < 0,01 - Norflurazon < 0,01 - Novaluron < 0,01 - Nuarimol < 0,01 - Ofurace < 0,01 - Omethoate < 0,01 - Oryzanil < 0,01 - Oxadiazon < 0,01 - Oxadixyl < 0,01 - Oxamyl < 0,01 - Oxidemeton-Methyl < 0,01 - Oxyfluorfen < 0,01 - Paclobrutazolo < 0,01 - Paraoxon Ethyl < 0,01 - Paraoxon Methyl < 0,01 - Paraquat < 0,01 - Parathion Ethyl < 0,01 - Parathion Methyl < 0,01 - Parathion-methyl (sum of Parathion-methyl and paraoxon-methyl < 0,01 Max 0.1 (176 expressed as Parathion-methyl - Pebulate < 0,01 - Pencicuron < 0,01 - Penconazole < 0,01 - Pendimethalin < 0,01 - Penoxsulam < 0,01 - Pentachloroaniline < 0,01 Page 12 of 17
Giancotti Rag. Giuseppe Commercio Ingrosso di Olii, Vini e Prodotti Tipici (@3720-12 - Pentacholoroanisol < 0,01 - Permethrin cis < 0,01 - Permethrin trans < 0,01 - Permethrin (sum of isomers < 0,01 Max 0.25 (155 - Phenmedipham < 0,01 - Phenthoate < 0,01 - Perthan < 0,01 - Phorate - Thimet < 0,01 - Phorate Oxon < 0,01 - Phorate Oxon Sulfone < 0,01 - Phorate Sulfone < 0,01 - Phorate (sum of phorate, its oxygen analogue and their sulfones < 0,01 Max 0.1 (176 expressed as phorate - Phosalone < 0,01 - Phosmet < 0,01 - Phosphamidon < 0,01 - Phoxim < 0,01 - Picolinafen < 0,01 - Picoxystrobin < 0,01 - Piperonyl Butoxide < 0,01 - Piridaben < 0,01 - Pirimicarb < 0,01 - Pirimicarb-Desmetyl < 0,01 - Pirimiphos Ethyl < 0,01 - Pirimiphos Methyl < 0,01 - Prochloraz < 0,01 - Procymidone < 0,01 - Profenofos < 0,01 - Profluralin < 0,01 - Prophoxydim < 0,01 - Promecarb < 0,01 - Prometon < 0,01 - Prometryn < 0,01 - Pronamide < 0,01 - Propachlor < 0,01 - Propamocarb < 0,01 - Propanil < 0,01 - Propaquizafop < 0,01 - Propargite < 0,01 - Propazine < 0,01 - Prometamphos < 0,01 - Propham < 0,01 - Propiconazole < 0,01 - Propoxur < 0,01 - (* Propyzamide < 0,01 - Proquinazid < 0,01 - Prosulfocarb < 0,01 Max 0.25 (192 - Prosulfuron < 0,01 Page 13 of 17
Giancotti Rag. Giuseppe Commercio Ingrosso di Olii, Vini e Prodotti Tipici (@3720-12 - Prothioconazolo < 0,01 - Prothiofos < 0,01 - Prothoate < 0,01 - Pymetrozine < 0,01 - Pyracarbolid < 0,01 - Pyraclostrobin < 0,01 - Pyraflufen-Ethyl < 0,01 - Pyrazophos < 0,01 - Pyrethrins < 0,01 - Pyridaben < 0,01 - Pyridaphenthion < 0,01 - Pyridate < 0,01 - Pyrifenox < 0,01 - Pyrimethanil < 0,01 - Pirimicarb-Desmethyl < 0,01 - Pyriproxifen < 0,01 - Quinalphos < 0,01 - Quinoxyfen < 0,01 Max 0.1 (196 - Quintozene < 0,01 - Quizalofop Ethyl < 0,01 - Quizalofop-P-Ethyl < 0,01 - Resmetrin < 0,01 - Rimsulfuron < 0,01 - Rotenone < 0,01 - Silafluofen < 0,01 - S-Ethyl dipropylthiocarbamate (EPTC < 0,01 - Simazine < 0,01 Max 0.05 (175 - Simetryn < 0,01 - Spinosad < 0,01 - Spinosyn D < 0,01 - Spirodiclofen < 0,01 - Spiromesifen < 0,01 - Spirotetramat < 0,01 - Spiroxamine < 0,01 - Sulfotep < 0,01 - SWEP < 0,01 - Sulprofos < 0,01 - TDCP < 0,01 - Tebuconazole < 0,01 - Tebufenozide < 0,01 - Tebufenpyrad < 0,01 - Tebupirimifos < 0,01 - Tebutam < 0,01 - Tecnazene < 0,01 - Teflubenzuron < 0,01 - Tefluthrin < 0,01 - Telodrin < 0,01 - Temefos < 0,01 Page 14 of 17
Giancotti Rag. Giuseppe Commercio Ingrosso di Olii, Vini e Prodotti Tipici (@3720-12 - TEPP < 0,01 - Tepraloxidim < 0,01 - Terbufos < 0,01 - Terbumeton < 0,01 - Terbuthylazina < 0,01 - Terbutryn < 0,01 - Tetrachlorvinphos < 0,01 - Tetraconazole < 0,01 Max 0.1 (195 - Tetradifon < 0,01 - Tetramethrin < 0,01 - TFM Tre-trifluorometil-4-nitrofenolo < 0,01 - Thiabendazole < 0,01 - Thiacloprid < 0,01 - Thiametoxam < 0,01 - Thiodicarb < 0,01 - Thiofanox < 0,01 - Thiometon < 0,01 - Thionazin < 0,01 - Thiophanate Methyl < 0,01 - Tralometrina < 0,01 - Thribenuron methyl < 0,01 - Tolclofos Methyl < 0,01 - Tolyfluanid < 0,01 - Transfluthrin < 0,01 - Triadimefon < 0,01 - Triadimenol < 0,01 - Triallate < 0,01 - Triamiphos < 0,01 - Triasulfuron < 0,01 - Triazamate < 0,01 - Triazophos < 0,01 - Tribenuron methyl < 0,01 - Trichlorfon < 0,01 - Triclhoronat < 0,01 - Triclopyr < 0,01 - Tricyclazole < 0,01 - Triexapac Ethil < 0,01 - Trifenilmetano < 0,01 - Trifloxystrobin < 0,01 - Triflumizolo < 0,01 - Triflumuron < 0,01 - Trifluralin < 0,01 - Thrisulfuron methyl < 0,01 - Triticonazol < 0,01 - Vamidothion < 0,01 - Uniconazole < 0,01 - Vinclozolin < 0,01 - Zoxamide < 0,01 Page 15 of 17
Giancotti Rag. Giuseppe Commercio Ingrosso di Olii, Vini e Prodotti Tipici (@3720-12 0000-02(* - in mg/kg o ppm - LOQ = 0,01 Cod. Met. / Metod: 0001-00 / UNI EN 1528-1:1997 + UNI EN 1528-2:1997 + UNI EN 1528-3:1997 + UNI EN 1528-4:1997 - (* Amitrole < 0.01 - (* AMPA < 0.01 - (* Chormequat < 0.01 - Cyromazin < 0.01 - (* Daminozide < 0.01 - (* Diethanolamine < 0.01 - (* Difenzoquat < 0.01 - (* Diquat < 0.01 - (* Ethepon < 0.01 - (* ETU < 0.01 - (* Fosetyl-Al < 0.01 - (* Glufosinate < 0.01 - Glyphosate < 0.01 - (* Hepa < 0.01 - (* Kasugamyzin < 0.01 - (* Maleic hydazide < 0.01 - (* Mepiquat < 0.01 - (* Morpholin < 0.01 - (* MPPA < 0.01 - (* N-Acetyl-AMPA < 0.01 - (* N-Acetyl-Glufosinate < 0.01 - (* N,N-Dimethylhydrazide < 0.01 - (* Nereistoxine < 0.01 - (* Paraquat < 0.01 - (* Perchlorate < 0.01 - (* Phosphonic Acid < 0.01 - (* PTU < 0.01 - (* Streptomycin < 0.01 - (* Triethanolamine < 0.01 - (* Trimesium < 0.01 (15 Reg. C.E.E. n. 2568/91, All. I; e succ. modifiche e integrazioni (29 E.E.C. Regulation No. 2568/91 Ann.I, and sub. amend. (155 Reg. (EC No 839/2008 (160 Reg. (EU No 441/2012 (161 Reg. (EC No 149/2008 (173 Reg. (EU No 293/2013 (174 Reg. (EU No 559/2011 (175 Reg. (EU No 310/2011 (176 Reg. (EU No 899/2012 (184 Reg. (EU No 251/2013 (192 Reg. (EU No 750/2010 (195 Reg. (EU No 34/2013 (196 Reg. (EU No 36/2014 (198 Reg. (EU No 777/2013 Page 16 of 17
RESULT Conformable to E.C.C. Regulation No. 2568/91 and following modifications and integrations. The Director of Laboratory Dr. Carmine Ventre Digitally signed document issued Page 17 of 17