Riferimenti del committente Lotto: 00003

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1 Rapporto di prova n : Data di emissione: 28/12/2017 Committente MOLITORIA SPILACETO SRL str. Calvese, NARNI TR Dati del campione Descrizione: Matrice: Dati di campionamento: Effettuato da: Committente Data: 09/11/2017 Riferimenti del committente Lotto: Farina di grano tenero antico Verna + Autonomia Origine: Italia cereali e derivati Data accettazione: 14/11/2017 Data inizio prove: 14/11/2017 Data fine prove: 27/12/2017 DON N.A. < 10 µg/kg 10 Lab 002/A036 rev RESIDUI LC/MS/MS e GC/MS/MS Permethrin (sum of isomers) I mg/kg ± Pirimiphos-Methyl A-I 0.17 mg/kg ± Abamectin (sum of Avermectin B1a, Avermectin B1b and delta- 8,9-Avermectin B1a as Avermectin B1a) Acephate Acequinocyl Acetamiprid Acetochlor Acibenzolar- S- methyl (sum of acibenzolar- S- methyl and acibenzolar acid as acibenzolar- S- methyl V Acibenzolar-S-methyl V Acifluorfen Aclonifen Acrinathrin Alachlor Aldicarb (sum of Aldicarb, its sulfoxide and its sulfone, expressed as Aldicarb) Aldicarb Aldicarb-Sulfone Aldicarb-Sulfoxide Aldoxycarb I-N Aldrin and Dieldrin (Aldrin and dieldrin combined expressed as dieldrin) Aldrin Dieldrin Allethrin Pagina 1 di 21

2 Ametoctradin Ametryn Aminocarb Amitraz(Amitraz including the metabolites containing the 2,4- Dimethylaniline moiety as amitraz) Amitraz 2,4 Dimethilaniline N-(2,4-DimethylPhenyl)-N'- Formamidine N-(2,4-DimethylPhenyl)- Formamide Anilazine Anthraquinone N.A. Atrazine Asulam Atrazine Desethyl Atrazine Desisopropyl Atrazine-Desethyl-Desisopropyl Azaconazole Azadirachtin Azimsulfuron Azinphos-ethyl Azinphos-methyl Azocyclotin and Cyhexatin (sum of Azocyclotin and Cyhexatin expressed as Cyhexatin) Azocyclotin Cyhexatin Azoxystrobin Barban Benalaxyl including other mixtures of constituent isomers including Benalaxyl-M (su of isomers) Bendiocarb Benfluralin Bensulfuron-Methyl Bentazone (sum of Bentazone, its salts and 6-hydroxy and 8-hydroxy bentazone as Bentazone) Bentazone 6-Hydroxy Bentazone 8-Hydroxy Bentazone Benthiavalicarb-isopropyl Pagina 2 di 21

3 Benzoximate Benzoylprop-ethyl Benzthiazuron Bifenazate Bifenox Bifenthrin Binapacryl A-F- Biphenyl C- Bispyribac Bitertanol Boscalid Bromacil Bromfenvinphos Bromocyclen Bromophos-Ethyl Bromophos-Methyl Bromopropylate Bromoxynil and its salts, expressed as Bromoxynil Bromoxynil octanoate Bromuconazole (sum of diasteroisomers) Bupirimate Buprofezin Butafenacil Butocarboxim Butoxycarboxim Buturon Butylate Cadusafos Captafol Captan (sum of Captan and THPI, expressed as Captan) Captan Tetrahydrophtalimide(cis-1,2,3,6) Carbaryl I-R Carbendazim and Benomyl (sum of Benomyl and Carbendazim expressed as Carbendazim) Carbendazim Benomyl Carbetamide Pagina 3 di 21

4 Carbofuran(sum of Carbofuran,Carbosulfan,Benfuraca rb, Furathiocarb and 3- OHCarbofuran as Carbofuran) I-N < mg/kg Carbofuran I-N < mg/kg Benfuracarb I < mg/kg Carbosulfan I < mg/kg Furathiocarb 3-Hydroxycarbofuran M < mg/kg Carbophenothion Carboxin Carfentrazone-Ethyl Chinomethionat Chlorantraniliprole Chlorbromuron Chlorbufam Chlordane (sum of cis- and transchlordane) Chlorfenapyr Chlorfenson Chlorfenvinphos Chlorfluazuron I-R Chloridazon Chlormephos Chlorobenzilate Chloroneb Chloropropylate Chlorothalonil Chlorotoluron Chloroxuron Chlorpropham D-R Chlorpyrifos Chlorpyrifos-methyl Chlorthal-Dimethyl Chlorthiamid Chlorthion Chlorthiophos I- Chlozolinate Cinosulfuron Pagina 4 di 21

5 Clethodim (sum of Sethoxydim and Clethodim including degradation products calculated as Sethoxydim) Clethodim Sethoxydim Clodinafop and its S-isomers and their salts expressed as Clodinafop-propargyl Clofentezine Clomazone Clomeprop Clopyralid Clothianidin Coumaphos Cyanazine Cyanofenphos Cyantraniliprole Cyazofamid Cycloate Cycloxydim Cycluron Cyflufenamid: sum of Cyflufenamid (Z-isomer) and its E- Cyfluthrin (cyfluthrin including other mixtures of constituent isomers (sum of isomers)) Cyfluthrin Beta Cyhalafop Cyhalofop-butyl Cymiazol Cymoxanil Cypermethrin (Cypermethrin including other mixtures of constituent isomers(sum of isomers)) Cypermethrin Alpha Cyproconazole Cyprodinil Cyprosulphamide Cyromazine Daminozide R Dazomet (Methylisothiocyanate resulting from the use of Dazomet and Metam) F-I- Pagina 5 di 21

6 DDT (sum of p,p -DDT, o,p -DDT, p-p -DDE and p,p -TDE (DDD) as DDT) 2,4'-DDD 2,4'-DDE 2,4'-DDT 4,4'-DDD 4,4'-DDE 4,4'-DDT DEET Deltamethrin Desmedipham Desmetryn Di-allate (sum of isomers) Diafenthiuron Dialifos I- Diazinon Dibrom Dicamba Dichlobenil Dichlofenthion Dichlofluanid Dichlorprop (Sum of dichlorprop (including dichlorprop-p), its salts, esters and conjugates) R Dichlorprop D-R Dichlorvos Diclobutrazol Diclofop (sum of Diclofop-methyl and Diclofop acid expressed as Diclofop-methyl) Diclofop-free acid Diclofop-methyl Dicloran Dicofol (sum of p,p' and o,p' isomers) Dicrotophos I- Diethofencarb Difenoconazole Difenoxuron Diflubenzuron Diflufenican Pagina 6 di 21

7 Dimefox Dimepiperate Dimethenamid (dimethenamid-p including other mixtures of constituent isomers(sum of isomers)) Dimethoate (sum of dimethoate and omethoate expressed as dimethoate) Dimethoate Omethoate Dimethomorph (sum of isomers) Dimoxystrobin Diniconazole (sum of isomers) Dinitramine Dinocap A- Dinoterb Dioxacarb Dioxathion (sum of isomers) Diphenamid Diphenylamine C-D-F-R Disulfoton (sum of Disulfoton, Disulfoton sulfoxide and Disulfoton sulfone as Disulfoton) Disulfoton Disulfoton sulfone Disulfoton sulfoxide Ditalimfos Dithianon Diuron Dodine Edifenphos Emamectin benzoate B1a, expressed as Emamectin Endosulfan (sum of alpha- and beta-isomers and Endosulfansulphate expressed as Endosulfan) Endosulfan alpha Endosulfan beta Endosulfan sulfate Endrin Endrin aldehyde EPN Pagina 7 di 21

8 Epoxiconazole EPTC Etaconazole Ethiofencarb Ethiofencarb-sulfone Ethiofencarb-sulfoxide Ethion Ethirimol Ethofumesate Ethoprophos I-N Ethoxyquin C- Ethoxysulfuron Etofenprox Etoxazole Etridiazole Etrimfos Famoxadone Famphur Fenamidone Fenamiphos (sum of Fenamiphosand its sulfoxide and sulfone expressed as I-N Fenamiphos N Fenamihos-Sulfone Fenamiphos-Sulfoxide Fenarimol Fenazaquin Fenbuconazole Fenbutatin-oxide Fenchlorphos (sum of Fenchlorphos and Fenchlorphos oxon expressed as Fenchlorphos) Fenchlorphos Fenchlorphos-Oxon Fenhexamid Fenitrothion Fenothiocarb Fenoxaprop-P Fenoxaprop-P-ethyl Fenoxycarb Fenpropathrin Pagina 8 di 21

9 Fenpropidin (sum of Fenpropidin and its salts expressed as Fenpropidin) Fenpropimorph Fenpyrazamina Fenpyroximate Fenson Fensulfothion I-N Fensulfothion-oxon I-N Fensulfothion-oxon-sulfone I-N Fensulfothion-sulfone I-N Fenthion (Fenthion and its oxigen analogue, theis sulfoxides and sulfone expressed as parent) Fenthion Fenthion-Sulfone Fenthion-Sulfoxide Fenthion-Oxon Fenthion-Oxon-Sulfone Fenthion-Oxon-Sulfoxide Fentin (Fentin including its salts, expressed as Triphenyltin cation) Fenuron Fenvalerate (any ratio of costituent isomers(rr, SS, RS & SR) including Esfenvalerate) Fenvalerate Esfenvalerate Fipronil (sum Fipronil + sulfone metabolite (MB46136) expressed as Fipronil) I < mg/kg Fipronil I < mg/kg Fipronil-Desulfinyl Fipronil-Sullfide Fipronil-Sullfone M < mg/kg Flamprop Flamprop-Isopropyl Flamprop-M-Methyl Flazasulfuron Flonicamid(Sum of Flonicamid, TNFA and TNFG expressed as Flonicamid) Flonicamid TFNA Pagina 9 di 21

10 TFNG Fluazifop-P(sum of all the isomers of fluazifop, its esters and its coniugates,express as fluazifop) Fluazifop Fluazifop-Butyl Fluazinam Fluazuron Flubendiamide Flubenzimine Flucycloxuron Flucythrinate (Flucythrinate including other mixtures of constituent isomers (Sum of isomers)) Fludioxonil Flufenacet Flufenoxuron Fluometuron Fluopicolide Fluopyram Flupyradifurone Fluquinconazole Flurochloridone Fluroxypyr (sum of Fluroxypyr, its salts, its esters, and its conjugates es Fluroxypyr) Fluroxypyr Fluroxypyr-1-Methylheptyl Ester Fluoxastrobin Flusilazole Flutolanil Flutriafol Fluxapyroxad Folpet (sum of Folpet and Phtalimide expressed as Folpet) Folpet Phtalimide Fonofos Forchlorfenuron R Formetanate: Sum of Formetanate and its salts expressed ad Formetanate (hydrochloride) Formothion Pagina 10 di 21

11 Fosthiazate I-N Fuberidazole Furalaxyl Furilazole Giberellic Acid R Halosulfuron Halosulfuron-methyl Haloxyfop(sum of Haloxyfop, its esters, salts and conjugates expressed as Haloxyfop) Haloxyfop Haloxyfop-2-Ethoxyethyl Haloxyfop-Methyl Hexachlorocyclohexane (HCH) sum of isomes, except the gamma isomer HCH alpha HCH beta HCH delta HCH gamma (Lindane) Heptachlor (sum of Heptachlor and Heptachlor epoxide expressed as Heptachlor) D- Heptachlor Heptachlor-Endo-Epoxide Heptachlor-Exo-Epoxide Heptenofos Hexachlorobenzene Hexaconazole Hexaflumuron Hexazinone Hexythiazox Imazalil Imazamox (Sum of Imazamox and its salts, expressed as Imazamox) Imazosulfuron Imibenconazole Imidacloprid Indoxacarb (Sum of Indoxacarb and its R enantiomer) Iodofenphos Ioxynil Iprobenfos Pagina 11 di 21

12 Iprodione Iprovalicarb Isazofos I-N Isocarbophos Isodrin Isofenphos Isofenphos-Methyl Isofenphos-Oxon Isoprocarb Isopropalin Isoprothiolane Isoproturon Isopyrazam Isoxaben Isoxaflutole (Sum of Isoxaflutole and its Diketonitrile-metabolite, as Isoxaflutole) Isoxaflutole Isoxaflutole Diketonitrile Isoxathion Kresoxim-Methyl Lambda-Cyhalothrin Lenacil Leptophos Linuron Lufenuron A-I-R Malathion (sum of Malathion and Malaoxon expressed as Malathion) Malathion Malaoxon Mancozeb Mandipropamid MCPA and MCPB (MCPA, MCPB including theis salts,esters anc conjugate as MCPA) MCPA MCPA-Methyl Ester MCPA-2-Ethylhexyl Ester MCPA-Butoxyethyl Ester MCPB Mecarbam Pagina 12 di 21

13 Mecoprop (sum of mecoprop-p and mecoprop expressed as mecoprop) Mepanipyrim Mephosfolan Mepronil Meptyldinocap Mesotrione Metaflumizone (sum of E- and Z- isomers) Metalaxyl and Metalaxyl-M (sum of isomers) Metamifop Metamitron Metazachlor Metconazole (sum of isomers) Methabenzthiazuron Methacrifos I- Methamidophos Methidathion Methiocarb (sum of Methiocarb and Methiocarb sulfoxide and sulfone, expressed as Methiocarb) Methiocarb Methiocarb-Sulfone Methiocarb-Sulfoxide Methomyl and Thiodicarb (sum of Methomyl and Thiodicarb expressed as Methomyl) Methomyl Thiodicarb Methomyl-oxyme Methoxychlor Methoxyfenozide Methyl-N-(3-hydroxyphenyl)- Carbamate Methyldymron Metobromuron Metolachlor and S-Metolachlor (sum of isomers) Metolcarb Metosulam Metoxuron Metrafenone Pagina 13 di 21

14 Metribuzin Metsulfuron-Methyl Mevinphos (sum of E- and Z- isomers) Mibemectin (sum of Milbemycin A4 and Milbemycin A3, expressed as Milbemectin) I-A-N Milbemycin A3 I-A-N Milbemycin A4 I-A-N Mirex Molinate Monocrotophos Monolinuron Monuron Myclobutanil N,N-Dimethyl-Hydrazide N,N-Dimethyl-Sulphamide Napropamide N.A. N.A. Naptalam Neburon Nicosulfuron Nitenpyram Nitrofen Nitrothal-Isopropyl Norfluazuron Novaluron Nuarimol Orthosulfamuron Oxadiargyl Oxadiazon Oxadixyl Oxamyl Oxamyl-Oxyme Oxycarboxin Oxydemeton-methyl (sum of Oxydemethon-methyl and Demethon-S-methylsulfon as Oxydemeton-methyl) Oxydemeton-Methyl Demeton-S-methyl Demeton-S-methylsulfone Oxyfluorfen Pagina 14 di 21

15 Paclobutrazol R Parathion-methyl (sum of Parathion-methyl and Paraoxonmethyl expressed as Parathionmethyl) Parathion Parathion-Methyl Paraoxon-Methyl Paraoxon Penconazole Pencycuron Pendimethalin Penoxsulam Pentachloroanisole Pentachlorophenol Penthiopyrad F-D- Perthane Phenkapton Phenmedipham I- Phenthoate Phorate (sum of Phorate, its oxygen analogue and their sulfones expressed as Phorate) Phorate Phorate-Oxon Phorate-Sulfone Phorate-Sulfoxide Phorate-Oxon-Sulfone Phorate-Oxon-Sulfoxide Phosalone Phosmet (Phosmet and Phosmetoxon expressed as Phosmet) Phosmet Phosmet Oxone Phosphamidon Phoxim Picloram Picoxystrobin Pinoxaden Piperonyl butoxide S Piperophos Pirimicarb Pagina 15 di 21

16 Pirimicarb-Desmethyl Pirimicarb-Desmethyl-Formamido Pirimiphos-Ethyl Pretilachlor Prochloraz(sum of Prochloraz and metabolites containing 2,4,6- Trichlorophenol moiety as Prochloraz) Prochloraz 2,4,6-Trichlorophenol Procymidone Profenofos Profluralin Profoxydim Prohexadone-calcium R Promecarb Prometon Prometryn Propachlor: oxalinic derivate of Propachlor, expressed as Propachlor Propamocarb (Sum of Propamocarb and its salts, expressed as Propamocarb) Propanil Propaquizafop Propargite Propazine Propetamphos Propham Propiconazole (mixture of isomers) Propoxur Propyzamide Proquinazid Prosulfocarb Prothioconazole: Prothioconazoledesthio (sum of isomers) Prothioconazole Prothioconazole-desthio Prothiofos Prothoate Pymetrozine Pyraclostrobin Pagina 16 di 21

17 Pyraflufen-ethyl Pyrazophos Pyrethrins Pyridaben Pyridafol Pyridalyl Pyridaphenthion Pyridate Pyrifenox Pyrimethanil Pyriproxyfen Quinalphos Quinclorac Quinoxyfen Quintozene (sum of Quintozene and Pentachloro-aniline expressed as Quintozene) Quintozene Pentachloroaniline Quizalofop, including Quizalofop-P Quizalofop p-ethyl Rimsulfuron Rotenone S421 Simazine Simetryn Spinetoram Spinosad (Spinosad, sum of Spinosyn A and Spinosyn D) Spirodiclofen Spiromesifen Spirotetramat and its 4 metabolite expressed as spirotetramat () Spirotetramat Spirotetramat BYI08330-enol Spirotetramat BYI enolglucoside Spirotetramat BYI Ketohydroxy Spirotetramat BYI monohydroxy Spiroxamine (sum of isomers) Sulcotrione Pagina 17 di 21

18 Sulfallate Sulfotep Sulfoxaflor Sulphur A- Sulprofos Tau-fluvalinate Tebuconazole Tebufenozide Tebufenpyrad Tebupirimfos Tecnazene F-R Teflubenzuron Tefluthrin Temephos Tepraloxydim Terbufos I-N Terbufos-Sulfon Terbufos-Sulfoxide Thiencarbazone-Methyl Terbumeton Terburol Terbuthylazine N.A. Terbuthylazine-Desethyl Terbutryn Tetrachlorvinphos Tetraconazole Tetradifon Tetramethrin Tetrasul Thiabendazole Thiacloprid Thiametoxam Thidiazuron Thiobencarb (4-chlorobenzyl methyl sulfone) Thiometon Thionazin I- Thiophanate-Methyl Thiram (expressed as Thiram) Tiocarbazil Pagina 18 di 21

19 Tolclofos-Methyl Tolylfluanid (Sum of tolylfluanid and dimethylaminosulfotoluidide expressed as Tolylfluanid) Tolylfluanid Dimethylaminosulfotoluidide Tralkoxidym (sum of the constituent isomers of Tralkoxydim) TralomethrIn Tranfluthrin Triadimefon and Triadimenol (sum of Triadimenol and Triadimenol) Triadimefon Triadimenol Tri-Allate Triamiphos Triasulfuron Triazamate Triazophos Tribenuron-methyl Trichlorfon Trichloronat Triclopyr Tricyclazole Tridemorph Trifloxystrobin Triflumizole: Triflumizole and metabolite FM-6-1 expressed as Triflumizole Triflumizole FM-6-1(N-(4-chloro-2- trifluoromethylphenyl)-npropoxyacetamidine) N.A. Triflumuron Trifluralin Triforine Trinexapac-Ethyl R Triticonazole Valifenalate Vamidothion Vinclozolin Zoxamide Pagina 19 di 21

20 1-Naphthol 1-Naphthylacetamide and 1- naphthylacetic acid (sum of 1-NAA and 1-NAD and its salts) N.A. R 1-Naphtylacetic acid R 1-Naphtylacetamide R 2,4-D (sum of 2,4-D, its salts, its esters and its conjugates, expressed as 2,4-D) D-R 2,4-D D-R 2,4-D methyl ester 2-Naphthyloxyacetic acid (BNOA) R 2-Nitroaniline N.A. 2-Phenylphenol C 2,4-DB (sum of 2,4-DB, its salts, its esters and its conjugates, expressed as 2,4-DB) 2,4-DB 2,4-DB methyl ester 2,4,5-T (sum of 2,4,5-T, its salts and esters, expressed as 2,4,5-T) 2,4,5-T 2,4,5-T methylester D-R 2,4,5-TP R- 2,6-Dichloro-4-Methylphenol 2,6-Dimethilaniline 3,4-Dichloroaniline 3,5-Dichloroaniline 3-Chloroaniline D-R 4,4'-Dibromobenzophenone 4-Bromo-2-Chlorophenol 4-CPA 4-Iodophenoxyacetic acid 4-phenylphenol 6-Benzylaminopurine R C R () Le prove contrassegnate dall'asterisco non sono accreditate da ACCREDIA. Legenda attività: I= Insetticida, A= Acaricida, F= Fungicida, R= Regolatori di crescita, N= Nematocidi, S= Sinergizzante piretrine, C= Conservanti post raccolta, D= Diserbanti, FU=Fumiganti, L=Limacida, N.A.= non applicabile, M= metabolita. Valori riferiti a: D.M.27/08/2004; Regolamento CEE/UE N. 396/2005; Regolamento CEE/UE N. 1881/2006. Per il parametro 1-Naphthylacetamide and 1-naphthylacetic acid (sum of 1-NAA and 1-NAD and its salts) il valore è espresso come 1-naphythlacetic acid. Per il parametro Dichlorprop (Sum of dichlorprop (including dichlorprop-p), its salts, esters and conjugates) il valore è espresso come Dichlorprop. () BYI08330-enol, BYI08330-ketohydroxy, BYI08330-monohydroxy, and BYI08330 enol-glucoside Pagina 20 di 21

21 I risultati riportati nel presente rapporto di prova si riferiscono unicamente al campione effettivamente sottoposto a prova. L'incertezza estesa è calcolata con un fattore di copertura pari a 2, con un intervallo di confidenza del 95%. I dati analitici non sono stati corretti per il recupero, gli analiti presentano recuperi in linea con quanto previsto dal metodo, ovvero tra %. Il presente rapporto di prova può essere riprodotto solo integralmente. La riproduzione parziale di questo rapporto di prova è ammessa solo dopo autorizzazione scritta del responsabile del laboratorio Water & Life Lab S.r.l. Il laboratorio Water & Life Lab S.r.l. è iscritto, con Decreto della Direzione Generale della Sanità numero 893 del 2 febbraio 2011, nel Registro della Regione Lombardia dei laboratori autorizzati ad effettuare analisi nell'ambito delle procedure di autocontrollo delle industrie alimentari al numero progressivo Responsabile di Laboratorio P.I. Enio Belotti Direzione Scientifica dott. Battista Nicoli Ordine dei Chimici Provincia di Bergamo Iscrizione n 95 Pagina 21 di 21