RAPPORTO DI PROVA n

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1 Pagina 1 di 14 ACIDI GRASSI LIBERI ±0,01 % di Acido 0,17 Oleico NUMERO DI PEROSSIDI ±0,2 meq O2 /kg 4,2 olio 01-C 0,8 (1) 23/03/ C 20 (1) 23/03/2016 ANALISI SPETTROFOTOMETRICA NELL'U.V. K232 1,59 ±0,09 10-C 2,5 (1) 23/03/2016 K268 0,092 ±0, C 0,22 (1) 23/03/2016 Delta K -0,003 ±0, C 0,01 (1) 11C 23/03/2016 MULTIRESIDUALE 2,4' DDD (Insecticides) ND 2,4' DDE (Insecticides) ND 2,4' DDT (Insecticides) ND 2,4,5-T (Herbicides) ND 2,4-D (Herbicides) ND 2,4-DB (Herbicides) ND 3-KETO CARBOFURAN ND 3-OH CARBOFURAN ND 4,4' DDD ND 4,4' DDE ND 4,4' DDT (Insecticides) ND ABAMECTINA (Insecticides) ND ACEPHATE (Insecticides) ND ACETAMIPRID (Insecticides) ND ACETOCHLOR (Herbicides) ND ACRINATHRIN (Insecticides) ND ALACHLOR (Herbicides) ND ALDICARB (Insecticides) ND ALDICARB SULFONE (Insecticides) ND ALDICARB SULFOXIDE ND ALDRIN (Insecticides) ND ALLETHRIN (Insecticides) ND ALLOXYDIM (Sodium) ND ALPHA BHC (Insecticides) ND AMETRYN (Herbicides) ND AMITRAZ (Insecticides) ND AMITROLE (Herbicides) ND ATRAZINE (Herbicides) ND AZACONAZOLE (Fungicides) ND AZADIRACHTIN (Insecticides) ND AZINPHOS-ETHYL (Insecticides) ND

2 Pagina 2 di 14 AZINPHOS-METHYL (Insecticides) ND AZOCYCLOTIN (Acaricides) ND AZOXYSTROBIN (Fungicides) ND BENALAXYL (Fungicides) ND BENDIOCARB (Insecticides) ND BENFLURALIN (Herbicides) ND BENFURACARB (Insecticides) ND BENOMYL (Fungicides) ND BENTAZONE (Herbicides) ND BENTHIAVALICARB ISOPROPYL (Fungicides) ND BENZOXIMATE (Acaricides) ND BENZOYLPROP-ETHYL (Herbicides) ND BENZTHIAZURON (Herbicides) ND BETA-BHC ND BETA-NOA (Grow Regulator) ND BHC (Fungicides) ND BIFENAZATE (Acaricides) ND BIFENOX (Herbicides) ND BIFENTHRIN (Insecticides) ND BINAPACRYL (Acaricides) ND BIORESMETHRIN (Insecticides) ND BIPHENYL (Fungicides) ND BITERTANOL (Fungicides) ND BOSCALID (Fungicides) ND BROMACIL (Herbicides) ND BROMOCYCLEN (Insecticides) ND BROMOPHOS ETHYL (Insecticides) ND BROMOPHOS METHYL (Insecticides) ND BROMOPROPYLATE (Acaricides) ND BROMOXYNIL (Herbicides) ND BROMUCONAZOLE (Fungicides) ND BUPIRIMATE (Fungicides) ND BUPROFEZIN (Insecticides) ND BUTACHLOR (Herbicides) ND BUTAFENACIL (Herbicides) ND BUTOXYCARBOXIM (Insecticides) ND BUTRALIN (Herbicides) ND BUTYLATE (Herbicides) ND CADUSAFOS (Insecticides) ND

3 Pagina 3 di 14 CAPTAFOL (Fungicides) ND CAPTAN (Fungicides) ND CARBARYL (Insecticide) ND CARBENDAZIM-total (Fungicides) ND CARBOFURAN (Insecticides) ND CARBOPHENOTHION (Insecticides) ND CARBOSULFAN (Insecticides) ND CARFENTRAZONE ETHYL (Herbicides) ND CARPROPAMID (Fungicides) ND CHINOMETHIONAT (Acaricides) ND CHLORANTRANILIPROLE (Insecticides) ND CHLORBENSIDE (Acaricides) ND CHLORDANE (Insecticides) ND CHLORFENAPYR (Insecticides/Acaricides) ND CHLORFENPROP METHYL (Herbicides) ND CHLORFENSON (Acaricides) ND CHLORFENVINPHOS (Insecticides) ND CHLORFLUAZURON (Insecticides) ND CHLORIDAZON (Herbicides) ND CHLOROBENZILATE (Acaricides) ND CHLORONEB (Fungicides) ND CHLOROPROPYLATE (Acaricides) ND CHLOROTHALONIL (Fungicides) ND CHLOROXURON (Herbicides) ND CHLOROXYNIL (Herbicides) ND CHLORPROPHAM (Growth regulator) ND CHLORPYRIFOS ETHYL (Insecticides) ND CHLORPYRIFOS METHYL (Insecticides) ND CHLORTHAL DIMETHYL (Herbicides) ND CHLORTHIAMID (Herbicides) ND CHLORTHION (Insecticides) ND CHLORTHIOPHOS (Insecticides) ND CHLORTOLURON (Herbicides) ND CHLOTIANIDIN (Insecticides) ND CHLOZOLINATE (Fungicides) ND CHROMAFENOZIDE (Insecticides) ND CINOSULFURON (Herbicides) ND CLETHODIM (Herbicides) ND CLIMBAZOLE (Fungicides) ND

4 Pagina 4 di 14 CLOFENTEZINE (Acaricides) ND CLOMAZONE (Herbicides) ND CLOMEPROP (Herbicides) ND CLORMEPHOS (Insecticides) ND COUMAPHOS (Insecticides) ND CYANAZINE (Herbicides) ND CYANOFENPHOS (Insecticides) ND CYANOPHOS (Insecticides) ND CYAZOFAMID (Fungicides) ND CYCLOATE (Herbicides) ND CYCLOSULFAMURON (Herbicides) ND CYCLOXYDIM (Herbicides) ND CYCLURON (Herbicides) ND CYFLUMETOFEN (Acaricides) ND CYFLUTHRIN (Insecticides) ND CYHALOFOP BUTHYL ND CYHEXATIN (Acaricides) ND CYMOXANIL (Fungicides) ND CYPERMETHRIN included alpha, betha, theta, zeta ND cypermethin (Insecticides) CYPROCONAZOLE (Fungicides) ND CYPRODINIL (Fungicides) ND CYROMAZINE (Acaricides) ND DAMINOZIDE (Growth regulator) ND DAZOMET (Fungicides/Herbicedes) ND DEET (Insecticides) ND DELTAMETHRIN (Insecticides) ND DEMETON-S-METHYL (Insecticides) ND DEMETON-S-METHYLSULPHON (Insecticides) ND DESMETRYN (Herbicides) ND DIAFENTHIURON (Acaricides/Insecticides) ND DIAZINON (Insecticides) ND DICHLOBENIL (Herbicides) ND DICHLOFENTHION (Insecticides, Nematicides) ND DICHLOFLUANID (Fungicides) ND DICHLORPROP (2,4 DP Herbicides) ND DICHLORPROP-P (Herbicides) ND DICHLORVOS (Insecticides) ND DICLOBUTRAZOL (Fungicides) ND

5 Pagina 5 di 14 DICLOFOP METHYL (Herbicides) ND DICLORAN (Fungicides) ND DICOFOL (Acaricides) ND DICROTOPHOS (Insecticides) ND DIELDRIN (Insecticides) ND DIETHOFENCARB (Fungicides) ND DIFENOCONAZOLE (Fungicides) ND DIFLUBENZURON (Insecticides) ND DIFLUFENICAN (Herbicides) ND DIMETHACHLOR (Herbicides) ND DIMETHENAMID (Herbicides) ND DIMETHOATE (Insecticides) ND DIMETHOMORPH (Fungicides) ND DIMOXYSTROBIN (Fungicides) ND DINICONAZOLE (Fungicides) ND DINITRAMINE (Herbicides) ND DINOCAP (Fungicides) ND DINOTEFURAN (Insecticides) ND DIOXABENZOFOS (Insecticides) ND DIOXACARB (Insecticides) ND DIOXATHION (Acaricides) ND DIPHENAMID (Herbicides) ND DIPHENYLAMINE (Fungicides) ND DISULFOTON (Insecticide) ND DITALIMFOS (Fungicides) ND DITHIANON (Fungicides) ND DIURON (Herbicides) ND DODINE (Fungicides) ND EDIFENPHOS (Fungicides) ND EMAMECTIN (Insecticides) ND ENDOSULFAN-total (Insecticides) ND ENDRIN (Insecticides) ND EPN (Insecticides) ND EPOXICONAZOLE (Fungicides) ND EPTC (Herbicides) ND ESFENVALERATE (Insecticides) ND ETACONAZOLE (Fungicides) ND ETHIOFENCARB (Insecticides) ND ETHION (Insecticides) ND

6 Pagina 6 di 14 ETHIRIMOL (Fungicides) ND ETHOFUMESATE (Herbicides) ND ETHOPROPHOS (Insecticides) ND ETHOXYQUIN (Fungicides) ND ETOFENPROX (Insecticides) ND ETOXAZOLE (Acaricides) ND ETRIDIAZOLE (Fungicides) ND ETRIMFOS (Insecticides) ND EXYTHIAZOX (Acaricides) ND FAMOXADONE (Fungicides) ND FENAMIDONE (Fungicides) ND FENAMIPHOS (Insecticides) ND FENARIMOL (Fungicides) ND FENAZAQUIN (Acaricides) ND FENBUCONAZOLE (Fungicides) ND FENHEXAMID (Fungicides) ND FENITROTHION (Insecticides) ND FENOBUCARB (Insecticides) ND FENOPROP (2,4,5 TP Herbicides) ND FENOTHIOCARB (Acaricides) ND FENOXAPROP ETHYL (Herbicides) ND FENOXYCARB (Insecticides) ND FENPROPATHRIN (Insecticides) ND FENPROPIDIN (Fungicides) ND FENPROPIMORPH (Fungicides) ND FENPYROXIMATE (Acaricides) ND FENSON (Acaricides) ND FENSULFOTHION (Insecticides) ND FENTHION-total, sum of Fenthion, Fenthion sulfoxide ND and Fenthion sulfone (Insecticides) FENURON (Herbicides) ND FENVALERATE (Insecticides) ND FIPRONIL (Insecticides) ND FLAZASULFURON (Herbicides) ND FLONICAMID (Insecticides) ND FLUAZIFOP-p-BUTYL (Herbicides) ND FLUAZINAM (Fungicides) ND FLUBENZIMINE (Acaricides) ND FLUCYTHRINATE (Insecticides) ND

7 Pagina 7 di 14 FLUDIOXONIL (Fungicides) ND FLUFENACET (Herbicides) ND FLUFENOXURON (Acaricides) ND FLUOPICOLIDE (Fungicides) ND FLUOPIRAM (Fungicide) ND FLUOTRIMAZOLE (Fungicides) ND FLUQUINCONAZOLE (Fungicides) ND FLUROXYPYR (Herbicides) ND FLUSILAZOLE (Fungicides) ND FLUTRIAFOL (Fungicides) ND FLUVALINATE (Insecticides) ND FOLPET (Fungicides) ND FONOFOS (Insecticides) ND FORMETANATE (Insecticides) ND FORMOTHION (Insecticides) ND FOSTHIAZATE (Nematicides) ND FURALAXYL (Fungicides) ND FURATHIOCARB (Insecticides) ND HALFENPROX (Insecticides) ND HALOXYFOP, including HALOXYFOP-P-METHYL ND (Herbicides) HCH, as sum of alfa and beta (Insecticides) ND HEPTACHLOR (Insecticides) ND HEPTACHLOR EPOXYDE (Insecticides) ND HEPTENOPHOS (Insecticides) ND HEXACHLOROBENZENE - HCB (Fungicides) ND HEXACONAZOLE (Fungicides) ND HEXAFLUMURON (Insecticides) ND HEXAZINONE (Herbicides) ND IMAZALIL (Fungicides) ND IMIDACLOPRID (Insecticides) ND INDAZIFLAM (Herbicide) ND INDOXACARB (Insecticides) ND IODOFENPHOS (Insecticides) ND IODOSULFURON (Herbicides) ND IOXYNIL (Herbicides) ND IPROBENFOS (Fungicides) ND IPRODIONE (Fungicides) ND IPROVALICARB (Fungicides) ND

8 Pagina 8 di 14 ISAZOFOS (Insecticides) ND ISODRIN (Insecticides) ND ISOFENPHOS (Insecticides) ND ISOFENPHOS METHYL (Insecticides) ND ISOPROCARB (Insecticides) ND ISOPROTHIOLANE (Fingicides, Insecticides) ND ISOPROTURON (Herbicides) ND ISOXAFLUTOLE (Herbicides) ND ISOXATHION (Insecticides) ND ISURON (Herbicides) ND KRESOXIM METHYL (Fungicides) ND LAMBDA CYHALOTHRIN (Insecticides) ND LENACIL (Herbicides) ND LINDANE (Insecticides) ND LINURON (Herbicides) ND LUFENURON (Insecticides) ND MALAOXON (Metabolite) ND MALATHION (Insecticides) ND MANDIPROPAMID (Fungicides) ND MCPA (Herbicides) ND MCPB (Herbicides) ND MCPP (Herbicides) ND MECARBAM (Insecticides) ND MEFENACET (Herbicides) ND MEPANIPYRIM (Fungicides) ND MEPHOSFOLAN (Insecticedes) ND MEPRONIL (Fungicides) ND MEPTYLDINOCAP (Fungicides) ND MESOSULFURON METHYL (Herbicides) ND METALAXYL (Fungicides) ND METAMITRON (Herbicides) ND METAZACHLOR (Herbicides) ND METCONAZOLE (Fungicides) ND METHACRIFOS (Insecticides) ND METHAMIDOPHOS (Insecticides) ND METHIDATHION (Insecticides) ND METHIOCARB (Insecticides) ND METHOMYL (Insecticides) ND METHOPRENE (Insecticides) ND

9 Pagina 9 di 14 METHOXYCHLOR (Insecticides) ND METHOXYFENOZIDE (Insecticides) ND METOBROMURON (Herbicides) ND METOLACHLOR (Herbicides) ND METOLCARB (Insecticides) ND METOXURON (Herbicides) ND METRAFENONE (Fungicides) ND METRIBUZIN (Herbicides) ND MEVINPHOS (Insecticides) ND MIREX (Insecticides) ND MOLINATE (Herbicides) ND MONOCROTOPHOS (Insecticides) ND MONOLINURON (Herbicides) ND MYCLOBUTANIL (Fungicides) ND NAA (1- Naphthalen acetic Acid) ND NAD (1-Naphthalen acethamide) ND NALED (Insecticides, Acaricides) ND NEBURON (Herbicides) ND NITENPYRAM (Insecticides) ND NITROFEN (Herbicides) ND NITROTHAL-ISOPROPYL (Fungicides) ND NORFLURAZON (Herbicides) ND NOVALURON (Insecticides) ND NUARIMOL (Fungicides) ND OFURACE (Fungicides) ND OMETHOATE (Insecticides) ND ORYZALIN (Herbicide) ND OXADIAZON (Herbicides) ND OXADIXYL (Fungicides) ND OXAMYL (Insecticides) ND OXYCARBOXIN (Fungicides) ND OXYFLUORFEN (Herbicides) ND PACLOBUTRAZOL (Growth Regulators) ND PARAOXON (Insecticides) ND PARAOXON METHYL (Insecticides) ND PARATHION ETHYL (Insecticides) ND PARATHION METHYL (Insecticides) ND PENCONAZOLE (Fungicides) ND PENCYCURON (Fungicides) ND

10 Pagina 10 di 14 PENDIMETHALIN (Herbicides) ND PENOXSULAM (Herbicides) ND PENTACHLOROANILINE (Fungicides) ND PENTACHLOROANISOLO (Fungicides) ND PERMETHRIN (Insecticides) ND PHENMEDIPHAM (Herbicides) ND PHENTHOATE (Insecticides) ND PHENYLPHENOL-2 (Fungicides) ND PHORATE (Insecticides) ND PHOSALONE (Insecticides) ND PHOSMET (Insecticides) ND PHOSPHAMIDON (Insecticides) ND PHTHALIDE (Fungicides) ND PICLORAM (Herbicides) ND PICOLINAFEN (Herbicides) ND PICOXYSTROBIN (Fungicides) ND PIPERONYL BUTOXIDE (Synergist) ND PIRIMICARB (Insecticides) ND PIRIMIPHOS ETHYL (Insecticides) ND PIRIMIPHOS METHYL (Insecticides) ND PRETILACHLOR (Herbicides) ND PROCHLORAZ (Fungicides) ND PROCYMIDONE (Fungicides) ND PROFENOFOS (Insecticides) ND PROFLURALIN (Herbicides) ND PROMECARB (Insecticides) ND PROMETON (Herbicides) ND PROMETRYN (Herbicides) ND PROPAMOCARB (Fungicides) ND PROPANIL (Herbicides) ND PROPARGITE (Acaricides) ND PROPAZINE (Herbicides) ND PROPHAM (Herbicides) ND PROPICONAZOLE (Fungicides) ND PROPOXUR (Insecticides) ND PROPYZAMIDE (Herbicides) ND PROQUINAZID (Fungicides) ND PROSULFOCARB (Herbicides) ND PROTHIOFOS (Insecticides) ND

11 Pagina 11 di 14 PROTHOATE (Insecticides, Acaricides) ND PYMETROZINE (Insecticides) ND PYRACLOSTROBIN (Fungicides) ND PYRAFLUFEN ETHYL (Herbicide) ND PYRAZOPHOS (Fungicides) ND PYRETHRINS (Insecticides) ND PYRIDABEN (Acaricides) ND PYRIDAPHENTHION (Insecticides) ND PYRIDATE (Herbicides) ND PYRIFENOX (Fungicides) ND PYRIMETHANIL (Fungicides) ND PYRIPROXYFEN (Insecticides) ND PYROQUILON (Fungicides) ND QUINALPHOS (Insecticides) ND QUINOXIFEN (Fungicides) ND QUINTOZENE (Fungicides) ND QUIZALOFOP (Herbicides) ND QUIZALOFOP ETHYL (Herbicides) ND ROTENONE (Insecticides) ND SILAFLUOFEN (Insecticides) ND SIMAZINE (Herbicides) ND SIMETRYN (Herbicides) ND SPINOSAD (Insecticides) ND SPIRODICLOFEN (Acaricides) ND SPIROMESIFEN (Insecticides) ND SPIROTETRAMAT (and metabolites) (Insecticides) ND SPIROXAMINE (Fungicides) ND SULFALLATE (Herbicides) ND SULFOTEP (Insecticides) ND TEBUCONAZOLE (Fungicides) ND TEBUFENOZIDE (Insecticides) ND TEBUFENPYRAD (Insecticides) ND TEFLUBENZURON (Insecticides) ND TEFLUTHRIN (Insecticides) ND TEPRALOXYDIM (Herbicides) ND TERBACIL (Herbicides) ND TERBUFOS (Insecticides) ND TERBUMETON (Herbicides) ND TERBUTHYLAZINE (Herbicides) ND

12 Pagina 12 di 14 TERBUTRYN (Herbicides) ND TETRACHLORVINPHOS (Insecticides) ND TETRACONAZOLE (Fungicides) ND TETRADIFON (Acaricides) ND TETRAMETHRIN (Insecticides) ND TETRASUL (Acaricides) ND THIABENDAZOLE (Fungicides) ND THIACLOPRID (Insecticides) ND THIAMETHOXAM (Insecticides) ND THIFLUZAMIDE (Fungicides) ND THIOBENCARB (Herbicides) ND THIODICARB (Insecticides) ND THIOFANOX (Insecticides) ND THIONAZIN (Insecticides) ND THIOPHANATE-METHYL (Fungicides) ND TIOCARBAZIL (Herbicides) ND TOLCLOPHOS-METHYL (Fungicides) ND TOLFENPYRAD (Insecticides) ND TOLYFLUANID (Fungicides) ND TOXAPHENE (Camphechlor) (Insecticide) ND TRALOMETHRIN (Insecticides) ND TRIADIMEFON (Fungicides) ND TRIADIMENOL (Fungicides) ND TRIALLATE (Herbicides) ND TRIAZOPHOS (Insecticides) ND TRICHLORPHON (Insecticides) ND TRICYCLAZOLE (Fungicides) ND TRIDEMORF (Fungicides) ND TRIFLOXYSTROBIN (Fungicides) ND TRIFLUMIZOLE (Fungicides) ND TRIFLUMURON (Insecticides) ND TRIFLURALIN (Herbicides) ND TRIFORINE (Fungicides) ND TRITICONAZOLE (Fungicides) ND UNICONAZOLE (Fungicides) ND VAMIDOTHION (Acaricides) ND VINCLOZOLIN (Fungicides) ND ZOXAMIDE (Fungicides) ND

13 Pagina 13 di 14 CONCLUSIONI: I parametri verificati risultano avere valori conformi a quanto previsto, per l'olio Extra Vergine di Oliva, dal Regolamento C.E.E. n.2568/91 della Commissione del 11/07/1991 in vigore dal 09/09/1991 e successive modifiche. Riferimenti Limiti (1) Reg CEE 2568/ /07/1991 GU CEE L248 05/09/1991, All I come modificato dal Reg UE 1830/2015 e dal Reg UE 1833/2015 GU UE L Note ND: Non rilevabile in quanto inferiore al LOD del metodo di prova 11C = In conformità con quanto riportato nel metodo di prova ufficiale, il risultato deve essere inteso come valore assoluto. U: Incertezza estesa, espressa nelle stesse unità di misura del risultato, calcolata adottando un fattore di copertura K=2 (se non diversamente specificato) per assicurare un livello di fiducia prossimo al 95%; oppure, per le prove microbiologiche e quelle delle fibre di amianto aerodisperse, intervallo di fiducia al livello di probabilità del 95%. Per le prove microbiologiche un risultato derivato da una conta sul campione, sulla sospensione iniziale o sulla prima diluizione compresa tra 4 e 9 (inclusi) viene considerato "stimato". LOD: Limite di rilevabilità, definito come la più bassa concentrazione dell'analita in un campione che può essere rilevata, ma non quantificata, nelle condizioni specificate. LOQ: Limite di quantificazione, la più bassa concentrazione dell'analita in un campione che può essere determinata, con accettabile precisione ed esattezza. R%: Recupero medio percentuale (non viene utilizzato per correggere il dato analitico sui fitofarmaci, sui metalli e sulle micotossine). En: Revisione "n" del Rapporto di Prova che identifica l'emendamento. L'Emendamento sostituisce ed annulla tutte le precedenti versioni del RdP. Le prove contrassegnate dall'asterisco (*) non rientrano nell'accreditamento ACCREDIA di questo Laboratorio : 01-C = Reg CEE 2568/ /07/1991 GU CEE L248 05/09/1991 All II Reg CE 702/ /06/2007 GU CE L161 22/06/ C = Reg CEE 2568/ /07/1991 GU CEE L248 05/09/1991 All III 10-C = Reg CEE 2568/ /07/1991 GU CEE L249 05/09/1991 All IX. Reg UE 299/ /03/ /03/2013 GU UE L90 28/03/ C = UNI EN : UNI EN : UNI EN : UNI EN :1997

14 Pagina 14 di 14 La descrizione del campione e/o eventuali ulteriori riferimenti allo stesso sono forniti dal committente. I risultati analitici riportati nel presente rapporto di prova si riferiscono unicamente al campione sottoposto a prova. La riproduzione parziale dello stesso deve essere autorizzata mediante approvazione scritta dal ns. Laboratorio. La documentazione utile alla rintracciabilità dei risultati analitici viene conservata in archivio per 4 anni. Rapporto di prova firmato digitalmente valido a tutti gli effetti di Legge ai sensi della normativa vigente. FINE RAPPORTO DI PROVA